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Top blue bar image Shannon's Nano Adventure
A Diary of Shannon's Experiences in the NEWT REU Program
 

ASU’s Amazing Lab

July 22nd, 2019 by Shannon Malinda

Our lab building(ISTB4) has so many interesting things that Roberto, his mom, my mom and I all came in on Saturday(the 29th of July). I meant to talk about this like three weeks ago, better late than never.

Every Wednesday, and Saturday the building puts on a movie open to the public, sometimes free, sometimes 5 dollars. We saw “50 Years of Hubble” for the anniversary of the telescope

Roberto, Me and my Mom

After the show we gave tours of our labs to our parents. Then we walked around the first floor of our building which has dinosaur bones/fossils, a space control area where people work with ASU’s space equipment, and much more.

We finished the day with the best ramen in Arizona at Shady Parks.

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A Week of Experiments

July 22nd, 2019 by Shannon Malinda

Last week we started experimenting! Up until this point we had been busy making our PNEDs(photothermal nanomaterial enabled desiccants) so I was very excited to start getting data. What we have seen so far is that the carbon black has not adsorbed as much water as the silica. This problem seems to be from the nano particles blocking the water adsorption. Oh well, we still have to see how the gold rods and cubes do.

The experiments take 10 hours to complete, most of that time is a lot of waiting. Since I am right behind Roberto’s lab he keeps me company.

The second part of our experiment is desorbtion which is done under a sun lamp, in Roberto’s lab. To prevent a sun burn I have to be all suited up.

The Baby is Born! A.K.A. a Lot of Labor Pains

July 15th, 2019 by Shannon Malinda

At the end of this week we finally finished making nano particles(our babies are born!)

The first of the last steps was to remove as much junk off of the top of the NP(nano particles) as I could. This took about a day of pipetteing.

When I collected as much of the liquid as I could they were all placed in the oven at 105 degrees to evaporate off the rest of the liquid.

When the particles where dry we took them out of the oven. The gold rods turned blue/green this is called blue shift theory and it means that they increased in energy!

 

They came a couple days late but boy am I so proud of them!

 

Also: Yes I am enjoying Jessica Jones, now that I’ve gotten through the second episode which was so dull!

Braxton Hicks Contractions A.K.A Almost done making NP

July 14th, 2019 by Shannon Malinda

Shaking nano particles + APTES + SiO_2 for optimal coating, using my own wrapping design. During this process we had to remove a bottle to see if they had been shaken sufficiently, which was awfully like trying to birth a baby. The hard part was getting it back in the wrapping, a job no doctor(or student) ever wants to do with a baby.

Beautiful view while waiting for the materials to be born

Getting the solar lamp set up for when we need to dry out the desiccant.

Moving the nest and getting it ready, got to have the humidity just right!

Parting note; Yes I have been watching Jessica Jones season 3

FT-IR(An Excuse To Play with Liquid Nitrogen)

July 5th, 2019 by Shannon Malinda

Today my mentor and I learned how to use the FT-IR machine. Wikipedia has this to say about the machine: “Fourier-transform infrared spectroscopy (FTIR) is a technique used to obtain an infrared spectrum of absorption or emission of a solid, liquid or gas.” We used this spectroscopy to see if APTES has attached to SiO_2. We are trying to use APTES as a link for the nano particles to attach to. Unfortunately we saw very low absorption that we think is APTES. This mean that the functionalization ether didn’t work or there is a very small amount that stuck. In our experiment we will see if that was enough APETS.


Me working with the FT-IR machine

The best part of using the FT-IR was that it needs liquid nitrogen to keep it cool, so even though the results weren’t what we had hoped for we(I) still had a blast. Sometimes all you need is a little child like wonder.

The Leidenfrost effect cleaning our dirty floor.

If you want to learn more this effect I recommend this video:

 

Half Way Done and Only Just Starting

July 4th, 2019 by Shannon Malinda

This week is the half way point in our REU program and I feel like I have only just started to get comfortable with the lab. This week we are finishing up making our gold rod nano particles.
Finishing up making gold nano particals

It’s a good thing we had the day off for Fourth of July because I don’t know when I was going to squeeze in my homework assignment(the power point is due Monday.) We will start our experiments next week and to keep on schedule we have started working on the weekend and poor Anjali is working through the holiday.

Scottsdale Water Campus

June 27th, 2019 by Shannon Malinda

This last Wednesday we went on a field trip to Scottsdale Water Campus. It was very interesting and surprisingly pretty. For those who don’t know, the city of Scottsdale is to the east of Phoenix and it is very wealthy.

The entrance to the water treatment plant.

We started the tour in a freezing cold room and got the talk about how great they are at what they do. I have to say, I had a migraine and therefore was not as impressed as I should have been. Apparently the site is the world’s largest Vasdose Zone groundwater-recharge well field, looking back that is pretty cool.

We were given ear buds and machines so we could hear the tour guild better in the loud rooms(did I say Scottsdale is rich?) then we finally got to leave the frigid cold!
Rows and rows of RO filters

The inside of one of the massive RO filters

 


The beautiful McDowell Mountains

Ariel’s Farewell Party

June 26th, 2019 by Shannon Malinda

Yesterday was my first mentor, Ariel’s, going away party. She was such a wonderful mentor and is a great friend. I wish her all the best in Los Vegas. I am honored to have been taught by her.

For the event we went to a restaurant which I had never been to called Cornish Pastie. The food was amazing and they had many different things I could eat. Being allergic to dairy I usually only have one or two things I can choose from, at that place I had four items! I didn’t know what to do with myself. I finally decided on the “vegan oggie” and boy it was an excellent choice.

Busy Busy Third Week

June 26th, 2019 by Shannon Malinda

Sadly mentor’s official last day was Friday.

Because of that this third week was spent helping her finish her projects, clean up her work space plus my own nano bubbles. I also made a how to video for our Moleaer nanobubble machine and an O&M Manual.

Check out the video out here:
https://drive.google.com/file/d/1GfFAyZ0xa_7LHYhMLiKjGv-tPAdBeN_j/view?usp=sharing

I wish I had had more time with it, but I only had three days to pull it together.
I am so excited to start working with Anjali next week!

The Great Leak

June 20th, 2019 by Shannon Malinda

I have survived the great leak of Tuesday 2019!

We came in Tuesday morning to discover that the Moleaer nanobubbles generator had spewed its water all over the lab. It had to be some time in the night because the water had already evaporated in spots, which was nice because it hid that is was our fault. Like a peer of mine said, “Flooding the lab is kind of like peeing your pants except a lot more people notice.”